Crystal structure of pentacaesium hexacosatelluridopentazirconate, Cs5Zr5Te26, a new polyanionic chalcogenometalate
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Synthesis and crystal structure of a new thiosemicarbzone, acenaphthenequinone thiosemicarbazone mono methanol
A new thiosemicarbzone compound was prepared by the reaction of acenaphthenequinone and thiosemicarbazide (1:1 molar ratio) in absolute methanol at 70°C. The crystal structure of this compound, acenaphthenequinone thiosemicarbazone mono methanol, was determined by X-ray crystallography. The unit cell parameters are as follows: a = 7.0384(14) Ǻ, b = 14.202(3) Ǻ, c = 14.270(3) Ǻ, β = 104.26(3)°. ...
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ژورنال
عنوان ژورنال: Zeitschrift für Kristallographie - New Crystal Structures
سال: 2003
ISSN: 2197-4578,1433-7266
DOI: 10.1524/ncrs.2003.218.3.287